Buchi Multivapo P-12 Instrukcja Użytkownika

093156 enMultivaporTM P-6/P-12Operation Manual

2 Safety10 Multivapor™ Operation Manual, Version ESymbol MeaningExplosive gases, explosive environmentHarmful to life-formsHot item, hot surfaceExplos

2 Safety11 Multivapor™ Operation Manual, Version ESymbol MeaningWear protective gogglesWear protective glovesAdditional user informationParagraphs sta

2 Safety12 Multivapor™ Operation Manual, Version E NOTICERisk of glass breakage by excessive strains.• Mount all glassware parts without strains• Ch

2 Safety13 Multivapor™ Operation Manual, Version E2.5.4 Safety elementsElectronics• The heating plate is equipped with an electronic over-temperatu

3 Technical data14 Multivapor™ Operation Manual, Version E3 Technical dataThis chapter introduces the reader to the Multivapor and its main componen

3 Technical data15 Multivapor™ Operation Manual, Version ETable 3-1: Items included in the Basic configurationProduct Order numberMultivapor platform

3 Technical data16 Multivapor™ Operation Manual, Version EMultivapor RotavaporIn contrast to the stand-alone configurations described before, this set

3 Technical data17 Multivapor™ Operation Manual, Version E3.1.2 Ordering matrixIn this section the items accessible by the ordering matrix are liste

3 Technical data18 Multivapor™ Operation Manual, Version EOrder number:MPx x1x x x x xProtective shieldProduct Order numberProtective shield P-6, P-1

3 Technical data19 Multivapor™ Operation Manual, Version EOrder number:MPx x x x x xCondenser assembly, P+G coatedProduct Order numberType S condense

3 Technical data20 Multivapor™ Operation Manual, Version EOrder number:MPx x x x x x xVacuum solutionProduct Order numberComprises a Woulff bottle to

3 Technical data21 Multivapor™ Operation Manual, Version ETable 3-5: Standard accessories (cont.)Product Order numberSample preparation rack P-6 4978

3 Technical data22 Multivapor™ Operation Manual, Version E3.1.4 Standard accessory glassware23 416785Fig. 3.1: Overview over the available BUCHI gla

3 Technical data23 Multivapor™ Operation Manual, Version E3.1.5 Optional accessoriesTable 3-8: Optional accessoriesProduct Order numberProtective sh

3 Technical data24 Multivapor™ Operation Manual, Version ETable 3-8: Optional accessories (cont.)Product Order numberF-100, 230 V; 50/60 Hz (400 W) 1

3 Technical data25 Multivapor™ Operation Manual, Version ETable 3-10: Range of application for the O-rings of the conical adaptersEPDM FKM FKKM PEEK

3 Technical data26 Multivapor™ Operation Manual, Version E3.3 Technical data overviewTable 3-11: Technical dataDimensions ( W×H×D) 270×400×400 mmWei

3 Technical data27 Multivapor™ Operation Manual, Version E3.4 Solvent tableTable 3-12: Solvent tableSolvent Formula Molar mass in g / molEvaporation

4 Description of function28 Multivapor™ Operation Manual, Version E4 Description of functionThis chapter explains the basic principle of the Multiva

4 Description of function29 Multivapor™ Operation Manual, Version Ea Evaporation areaThe solvent is heated by means of a heating plate. Horizontal or

Table of contents3 Multivapor™ Operation Manual, Version ETable of contents1 About this manual . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 Description of function30 Multivapor™ Operation Manual, Version Econdenser cannot cope with the amount of vapor produced. During operation of the M

4 Description of function31 Multivapor™ Operation Manual, Version E4.1.5 Rear connections of the Multivapor12a Mains supplyb Main fuseFig. 4.6: Rea

4 Description of function32 Multivapor™ Operation Manual, Version E4.3 Crystal rack1The crystal rack a is fixed onto the heating plate and operates a

4 Description of function33 Multivapor™ Operation Manual, Version E4.5 Blank adapters (optional)Fig. 4.10: Blank adaptersIf less than the maximum nu

4 Description of function34 Multivapor™ Operation Manual, Version E4.8 Sample transfer plateAs the test tubes are tightly fixed to the transfer plate

4 Description of function35 Multivapor™ Operation Manual, Version E4.10 Protective shield (optional)The protective shield protects the user from spl

4 Description of function36 Multivapor™ Operation Manual, Version E4.12 High-boiling solvents - Woulff bottle (optional)To prevent boiling retardati

4 Description of function37 Multivapor™ Operation Manual, Version E4.14 Connection to a rotary evaporator (optional)Fig. 4.19: A resource-sharing co

5 Putting into operation38 Multivapor™ Operation Manual, Version E5 Putting into operationThis chapter describes the installation of the Multivapor

5 Putting into operation39 Multivapor™ Operation Manual, Version E5.3 Commissioning the Multivapor basic instrument5.3.1 Commissioning the crystal

Table of contents4 Multivapor™ Operation Manual, Version E4 Description of function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 Putting into operation40 Multivapor™ Operation Manual, Version E5.3.2 Assembling the Woulff bottle (optional)Fig. 5.22: Assembling the Wou

5 Putting into operation41 Multivapor™ Operation Manual, Version E5.4 Glass assembly NOTICERisk of glass breakage by excessive strains.• Mount all

5 Putting into operation42 Multivapor™ Operation Manual, Version E5.5 Tube connections5.5.1 Cooling waterWhen connecting the white cooling water tu

5 Putting into operation43 Multivapor™ Operation Manual, Version E5.5.2 Vacuum tubesWhen establishing the vacuum tube (red rubber) connections proce

5 Putting into operation44 Multivapor™ Operation Manual, Version E5.6 Commissioning the Multivapor-Rotavapor editionThe T-piece is inserted between

5 Putting into operation45 Multivapor™ Operation Manual, Version Ethe corresponding seals. The adapter seals have to be exchanged regularly. The corr

6 Operation46 Multivapor™ Operation Manual, Version E6 OperationThis chapter explains the operating elements and possible operating modes. It gives i

6 Operation47 Multivapor™ Operation Manual, Version E6.1.1 Selecting a preset temperatureA preset temperature setting ensures that the heating bath t

6 Operation48 Multivapor™ Operation Manual, Version E6.2 Sample preparation6.2.1 Heating up the instrumentDistilled water is added to each glass cyl

6 Operation49 Multivapor™ Operation Manual, Version E• Screw the adapter onto the tube. • Place the sample tube into the transfer plate. Make sure

Table of contents5 Multivapor™ Operation Manual, Version E6 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6 Operation50 Multivapor™ Operation Manual, Version E6.3 Selecting the distillation conditionsTo achieve optimal distillation conditions, the distill

6 Operation51 Multivapor™ Operation Manual, Version E6.4 DistillationBefore operating the system, the following conditions must be fulfilled:• All el

6 Operation52 Multivapor™ Operation Manual, Version E6.5.2 Pressure gradients (V-855)Setting the pressure manually to the boiling point involves the

6 Operation53 Multivapor™ Operation Manual, Version Etend to foam or splash. A preceding terrace at high pressure for approx. 10 min usually significan

6 Operation54 Multivapor™ Operation Manual, Version Eheating plate and the ambient temperature.6.7 When the distillation “dies out”When the distillat

7 Maintenance55 Multivapor™ Operation Manual, Version E7 MaintenanceThis chapter provides instructions on all required maintenance to keep the instru

7 Maintenance56 Multivapor™ Operation Manual, Version E7.3.2 Replacing the tube adapter seals1 2a Use the Multivapor tool for removing the insert of

7 Maintenance57 Multivapor™ Operation Manual, Version E7.3.4 Cleaning the vacuum cover and replacing the corresponding O-rings NOTICERisk of componen

7 Maintenance58 Multivapor™ Operation Manual, Version ETo remove the crystal rack for cleaning, proceed as follows:1Pull and hold the locking device.2

7 Maintenance59 Multivapor™ Operation Manual, Version ENOTEScrew the lid only hand-tight as overtightening may break the glass cylinders. Test the tig

1 About this manual6 Multivapor™ Operation Manual, Version E1 About this manualThis manual describes the Multivapor P-6 and P-12 and provides all in

8 Troubleshooting60 Multivapor™ Operation Manual, Version E8 TroubleshootingThe following chapter describes how to resume operation of the instrument

8 Troubleshooting61 Multivapor™ Operation Manual, Version ETable 8-1: General malfunctions and their remedyMalfunction Possible cause RemedyDistillati

9 Shutdown, storage, transport and disposal62 Multivapor™ Operation Manual, Version E9 Shutdown, storage, transport and disposalThis chapter instruc

9 Shutdown, storage, transport and disposal63 Multivapor™ Operation Manual, Version E1. Product (Model): ... 2

10 Spare parts64 Multivapor™ Operation Manual, Version E10 Spare partsThis chapter lists spare parts, accessories, and optional extras, including al

10 Spare parts65 Multivapor™ Operation Manual, Version E10.2 Evaporation unit11057259Table 10-2: Evaporation unit P-6Product Order numberQuick lock

10 Spare parts66 Multivapor™ Operation Manual, Version E11057259Table 10-3: Evaporation unit P-12Product Order numberQuick lock nut 11057259Vacuum co

10 Spare parts67 Multivapor™ Operation Manual, Version E10.3 Adapter setsTable 10-4: Adapter set P-6Product Order numberSet of 12 adapter springs 48

10 Spare parts68 Multivapor™ Operation Manual, Version E10.4 Condenser assembliesTable 10-6: Condenser assembly type SProduct Order numberSet of 5 G

10 Spare parts69 Multivapor™ Operation Manual, Version E10.5 Various glass partsTable 10-8: Rotavapor connectionProduct Order numberT-piece with SVL

1 About this manual7 Multivapor™ Operation Manual, Version E1.3 AbbreviationsChemicals:EPDM: EthylenepropylenedimonomerFEP: Combination of tetrafl

10 Spare parts70 Multivapor™ Operation Manual, Version ETable 10-10: Sample vesselsProduct Order numberSet of 25 round bottom BUCHI P-12 sample vesse

10 Spare parts71 Multivapor™ Operation Manual, Version E10.6 MiscellaneousTable 10-12: DocumentationProduct Order number Product Order numberInstall

10 Spare parts72 Multivapor™ Operation Manual, Version ETable 10-15: Vacuum solutionsProduct Order numberVacuum Controller V-850 47231Vacuum Controll

11 Declarations and requirements73 Multivapor™ Operation Manual, Version E11 Declarations and requirements11.1 FCC requirements (for USA and Canada

11 Declarations and requirements74 Multivapor™ Operation Manual, Version E11.2 Declaration of conformity

093156 en 1112 / Technical data are subject to change without notice/ Quality Systems ISO 9001The English version is the original language version and

2 Safety8 Multivapor™ Operation Manual, Version E2 SafetyThis chapter highlights the safety concept of the Multivapor and contains general rules of b

2 Safety9 Multivapor™ Operation Manual, Version E2.4 Safety warnings and safety signals used in this manualDANGER, WARNING, CAUTION and NOTICE are st