Buchi DuMaster D-480 Instrukcja Użytkownika Strona 1

Przeglądaj online lub pobierz Instrukcja Użytkownika dla Urządzenia pomiarowe Buchi DuMaster D-480. BUCHI DuMaster D-480 User Manual Instrukcja obsługi

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Podsumowanie treści

Strona 1 - Operation Manual

DuMaster D-480Operation Manual11593626 en

Strona 2

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 10 Column properties (Dialog) ...

Strona 3 - Copyright Note 3

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 100 Prioritizing urgent samples Via Edit > Swap you

Strona 4

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 101 The following import options are available:  Imp

Strona 5 - Contents

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 102 Performing other administrator tasks Target group

Strona 6 - Contents 6

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 103 Modifying the registration Dialog: "Product r

Strona 8 - Contents 8

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Strona 9 - Contents 9

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 106 Setting up and starting up the instrument Target

Strona 10 - Contents 10

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 107 Rules for first-time start-up First-time start-u

Strona 11 - Contents 11

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 108  Room temperature should be constant.  Analy

Strona 12

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 109 Category Type Part of initial equipment Carrier

Strona 13 - General

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 11 Statistics > Clear statistic (Command) ...

Strona 14 - Revision history

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 110  Filling the drying tube (on page 234).  Fil

Strona 15 - About this document

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 111 Peripherals  A PC must be connected. It is ess

Strona 16 - Display conventions

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 112 Detail of the rear The following picture shows a

Strona 17 - Basic security settings

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 113 Removing the furnace transport protection Procee

Strona 18

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 114  Push the left side door open from inside (mag

Strona 19 - Warning: residual risks

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 115 CO2 intake pressure CO2 intake pressure is set a

Strona 20 - Instrument casing

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 116 Shutting down the instrument Target group Person

Strona 21 - Waste gas lines

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 117 Shutting the instrument down for short measuring

Strona 22 - Meaning of the warning signs

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Heating up the furnace / checking parameters 118  In case the analyzer has to be transported, m

Strona 23 - Knowledge and skills

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with basic knowledge of chemistry and experience with laboratory work, e. g. ch

Strona 25 - Changing mode

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 120 Measurement settings Target group Personnel with basic knowledge of chem

Strona 26 - Filling reaction tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 121 Defining keywords for blank and conditioning samples Keywords Names of b

Strona 27 - Filling the drying tube

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 122  Click Close to close the dialog. Required substances Different amino

Strona 28

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 123 Specifying the computation method for blank value and daily factor Defin

Strona 29 - Product description

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 124  ... switch off a signal, uncheck the appropriate checkbox.  Click O

Strona 30 - 3 - Product description 30

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 125 Preparing samples Target group Personnel with basic knowledge of chemist

Strona 31 - Technical specifications

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 126 Sample preparation instructions Samples with potential risks Various sam

Strona 32 - Ambient conditions

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 127 The result will be that the nitrogen content is well measurable and you

Strona 33 - Instrument design

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 128 Packing fatty, humid and non-pelletizeable solid samples - packing with

Strona 34 - Front view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 129 Preparing measurement work Target group Personnel with basic knowledge o

Strona 35 - Furnace section

Operation Manual D-480 ©BÜCH Labortechnik AG Purpose This chapter contains general topics of the document. In this chapter Revision history ...

Strona 36 - Rear view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 130 Software usage rules Software usage rules Observe th following rules in

Strona 37 - Right side view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 131  The carrier gas is reactivated and the furnaces are heated up to thei

Strona 38 - Left side view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 132  Open the "Methods" dialog in the operating software by sele

Strona 39 - Top view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 133 Copy methods Defining custom methods The existing method can be copied

Strona 40

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 134  ... "Auto-decrement the number in the sample name": Works t

Strona 41 - CHAPTER 4

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 135  This closes the dialog and the samples are swapped in the sample memo

Strona 42

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 136 Performing measurement work Target group Personnel with basic knowledge

Strona 43 - Functional units

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 137 Values for oxygen dosing Meaning of oxygen dosing The following illustra

Strona 44 - dosing system (I)

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 138 Animal feed, approx. 500 mg medium fat content 50 mgFeed 250 ml/min, 1

Strona 45

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 139 When is routine measuring work necessary? You must perform routine measu

Strona 46

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 14 Revision history List of modifications in this document up to now Date Modification

Strona 47

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 140  Save the data or print them out. See Data backup and printing (on pag

Strona 48 - Introduction

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 141 Definitions Routine measuring work comprises the following activities: 

Strona 49

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 142  Measure a maximum of 50 real samples.  At the end of the series, me

Strona 50 - Setting device parameters

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 143 Checklist Go through the following list:  Were the results of a blank

Strona 51 - Instrument equipment

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 144  The N integral values should be between 10 and 50 after stabilization

Strona 52

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 145  Name: Blnk  Weight: 1 mg  Click Method in the line of the appropr

Strona 53

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 146  Allocate the daily factor to the real samples in the sample view (tex

Strona 54

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 147  Click OK. "Standard tolerance monitoring" is now enabled.

Strona 55 - Calibration formulae

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 148 Preparing measuring data for evaluation Target group Personnel with basi

Strona 56 - Routine measuring work

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 149 Configuring the sample view Configuring the sample view Proceed as follo

Strona 57 - Daily factor determinations

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 15 About this document Status of the operating instructions The status of the operating i

Strona 58 - Daily factor

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 150 Saving the sample view Saving the sample view Proceed as follows:  Ope

Strona 59

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 151  You can generate statistical data manually. In this case, the user co

Strona 60

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 152 Mean value The mean value of "n" element concentrations is com

Strona 61 - Software user interface

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 153 Single peaks In general a single peak looks as follows: Superimposed pe

Strona 62 - Sample view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 154 Manual integratability Regarding the integratability there are certain d

Strona 63 - Color coding

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 155  Click and mark the peak end in the same way as described in the pre

Strona 64 - Combi view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 156  The peak area was entered in the corresponding cell in the sample vie

Strona 65

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 157 Setting the size of the graph with the mouse Proceed as follows:  Drag

Strona 66 - Calibration view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 158 Data backup and printing Why backup and print data? The measuring data

Strona 67 - Status view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 159 Overview of export and import file formats Export and import The analysi

Strona 68

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 16 Display conventions Before you start using this guide, it is important to understand t

Strona 69 - Right mouse button function

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 160  Edit the imported data as required and save them when you are finishe

Strona 70 - Further functions

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 161 Working with documents Target group Personnel with basic knowledge of ch

Strona 71 - Copyright Note 71

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 162 Creating new documents Usual procedure Usually, one document is created

Strona 72 - Copyright Note 72

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 163 Swap samples Proceed as follows:  Open the "Swap samples" di

Strona 73 - 21 CFR Part 11 functionality

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 164  A message appears which informs that the coefficients included in the

Strona 74 - Versioning

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 165 Importing documents Importing documents Proceed as follows:  Open the

Strona 75 - Work performed by the system

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 166 Checking documents for authenticity What signature is checked? Only thos

Strona 76 - Requirements for operation

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Strona 77 - Configure analyzer

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 168 Important information about maintenance Target group Personnel au

Strona 78 - Defining logon timeout

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 169 Maintenance work to be performed by the customer Note Observe tha

Strona 79 - Creating new sections

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel working with the instrument. Purpose This section describes basic safety rules

Strona 80

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 170 Viewing the status of maintenance intervals Viewing maintenance i

Strona 81 - LIMS export settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 171 Status view message If the maximum number of measurements is reac

Strona 82

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 172 Safety instruction Strictly observe the safety instruction &quo

Strona 83 - Granting authorizations

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 173  Baking out tubes to remove moisture and contaminations from th

Strona 84

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 174 Safety instruction Strictly observe the safety instruction &qu

Strona 85 - Defining interfaces

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 175 Performing the calibration Target group Personnel authorized by B

Strona 86

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 176 Viewing list of defined factor, monitor and standard samples View

Strona 87 - Dialog details

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 177 Viewing calibration coefficients Viewing calibration coefficients

Strona 88 - Editing analysis data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 178 Process The section is divided into the following phases:  Prep

Strona 89

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 179  Set oxygen dosing parameters (method) for conditioning and cal

Strona 90 - Performing checks

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 18 Working with the operating instructions Operating the analyzer Read th

Strona 91

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 180  Click OK to save your settings and close the dialog. The "

Strona 92 - Viewing the logbook

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 181  If deleting has not had the desired effect, you can undo it. T

Strona 93 - Working with the database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 182 Assessing the calibration curves Calibration curve display in the

Strona 94 - Database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 183 The following table explains the characteristics relating to the

Strona 95 - Database backup

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 184

Strona 96 - Reorganize database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 185 Calibration tables Target group Personnel authorized by BÜCHI Lab

Strona 97

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 186 Calibration table for nitrogen calibration Suggestion The followi

Strona 98

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 187 Replacing the ash crucible Target group Personnel authorized by B

Strona 99 - Sleep/wake-up behavior

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 188 Purpose and frequency of crucible replacement Why replace the ash

Strona 100

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 189 Furnace area The following picture shows the details of the furna

Strona 101 - Optimizing data evaluation

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 19  Read the instructions on the individual chemicals in the safety dat

Strona 102

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 190  Press the post combustion tube plug (1) and the combustion tub

Strona 103 - Printer setup

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 191  Place the ash crucible in the tube rack into the vent or else

Strona 104

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 192  Insert the new ash crucible into the combustion tube (4).  P

Strona 105 - CHAPTER 6

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 193 Replacing sealing elements Target group Personnel authorized by B

Strona 106

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 194 When to replace sealing elements What sealing elements are used?

Strona 107 - General requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 195 Visual o-ring/quad ring check You can tell when o-rings or quad r

Strona 108 - Specific requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 196 Ball valve maintenance Target group Personnel authorized by BÜCHI

Strona 109 - Start-up

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 197 Removing and dismantling the ball valve Note The following sectio

Strona 110 - Connecting peripherals

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 198 Furnace area The following picture shows the details of the furna

Strona 111 - Configuring the balance

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 199 Furnace area The following picture shows the details of the furna

Strona 112

ImprintProduct Identification: Operation Manual, DuMaster D-480 11593626 enBÜCHI Labortechnik AG Meierseggstrasse 40 Postfach CH-9230 Flawil 1E-Mail: q

Strona 113

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 20  Contact with the substances may lead to chemical burns or poisoning

Strona 114 - Default instrument settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 200 Phase 4: Dismantling the ball valve Please observe the following

Strona 115 - Flow rate

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 201  Remove the ball and top half shell by means of the "knock

Strona 116 - Shutting down the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 202 Process The section is divided into the following phases:  Clea

Strona 117 - Procedure

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 203 Phase 2: Assembling the ball valve Proceed as follows:  Slighly

Strona 118 - Safety instruction

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 204 Furnace area The following picture shows the details of the furna

Strona 119 - Using the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 205 Maintaining the Ni flap and the O2 lance Target group Personnel a

Strona 120 - Measurement settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 206 Purpose and frequency of maintaining the Ni flap and O2 lance Why

Strona 121 - Viewing the list

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 207 Furnace area The following picture shows the details of the furna

Strona 122

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 208 Phase 2: Removing the Ni flap (continued) Proceed as follows: 

Strona 123

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 209 Installing the Ni flap Note The following section is a continuati

Strona 124 - Configuring error handling

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 21  Front door  Left side door  Rear wall  Instrument cover. The

Strona 125 - Preparing samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 210  Place the ungreased seal on the combustion tube connection (3)

Strona 126 - Determining sample weight

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 211 Process This maintenance work is always carried out together with

Strona 127 - Packing samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 212 Installing the O2 lance Proceed as follows:  Pull on the lance

Strona 128

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 213 Removing, cleaning and installing the quartz glass bridge Target

Strona 129 - Preparing measurement work

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 214 Removing the quartz glass bridge Process The section is divided i

Strona 130 - Waking up the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 215 When to clean the quartz glass bridge The quartz glass bridge mus

Strona 131 - Defining custom methods

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 216 Note: When you close a ground-in ball-and-socket joint, you must

Strona 132 - Defining the Kjeldahl factor

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 217 Removing, cleaning and installing the carousel Target group Perso

Strona 133 - Settings for sample input

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 218 Removing, cleaning and installing the carousel Purpose of cleanin

Strona 134 - Prioritizing urgent samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 219  Lift off the ring at the pilots.  Clean the plastic top se

Strona 135 - What can you optimize?

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 22 Warning signs on the analyzer Warning sign furnace The following pictu

Strona 136 - Performing measurement work

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 220 Emptying and filling reaction tubes Target group Personnel author

Strona 137 - Values for oxygen dosing

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 221 Emptying reaction tubes Requirements: Before starting work, the f

Strona 138 - Performing measurements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 222 Filling the combustion tube Note Note the following rules:  O

Strona 139

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 223  Pour the recommended amounts of copper oxide (CuO) and corundu

Strona 140 - Overview

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 224  Insert the wire mesh ronde.  Fill the chemicals through the

Strona 141

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 225 Filling the reduction tube Proceed as follows:  Furnish both pl

Strona 142 - Checklist

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 226 Removing/installing and conditioning the reaction tubes In this s

Strona 143 - Background

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 227 Removing the reaction tubes from the furnace Process The section

Strona 144 - Determining blank values

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 228 Top view furnace The following picture shows a top view of the fu

Strona 145 - Determining the daily factor

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 229  Remove the quartz glass bridge. Hold the quartz glass bridge a

Strona 146

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 23 Warning: changes to the instrument Safe instrument The analyzer is des

Strona 147 - Stopping continuous analysis

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 230 Top view furnace The following picture shows a top view of the fu

Strona 148

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 231 Note: When you close the ground-in ball-and-socket joints, you mu

Strona 149 - Configuring the sample view

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 232  Close the front door. Phase 2: Conditioning the reaction tube,

Strona 150 - Generating statistical data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 233 Filling, removing and installing the absorption and drying tubes

Strona 151 - Statistical data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 234 Filling the drying tubes Note Note the following rules:  Observ

Strona 152 - Manual peak integration

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 235 Drying tube filling (large) The following picture shows the filli

Strona 153 - Melted peaks

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 236 Notes regarding further operation The drying tube fillings must b

Strona 154 - Integration of single peaks

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 237 To prepare the instrument for maintenance work follow the instruc

Strona 156 - Configuring the graph view

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Strona 157 - Display print preview

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 24 Required personal safety equipment Protective glasses You require prot

Strona 158 - Data backup and printing

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 240 Interpreting PC error messages Software reaction to errors When an e

Strona 159 - Export and import

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 241 Interpreting combustion module error messages and troubleshooting Th

Strona 160 - Exporting LIMS data

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 242 Performing a leak test Purpose of the leak test The leak test checks

Strona 161 - Working with documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 243 Leak test procedure Process The execution of the leak test takes pla

Strona 162 - Editing documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 244 F7 + F8 Furnace transformer 15 A Process The section is divided in

Strona 163 - Finding documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 245 Phase 2: Remove and check fuse Proceed as follows:  If a part of t

Strona 164 - Inserting data

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 246  The electrical section is now visible.  Pull out the fuse hol

Strona 165 - Signing documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 247  Plug the protective earth conductor back into the rear wall. 

Strona 166 - Checking a signature

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 248 Reacting to a power failure Open document An open document is not lo

Strona 167 - Maintaining the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 249  Perform a leak test by selecting Options > Diagnostics > Le

Strona 168

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 25 Damaged base panel Please observe the following instruction: Caution

Strona 169 - Recommendation

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 250 Checking air-tightness of instrument Proceed as follows:  Perform

Strona 170

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 251  Weigh the sample If the weight is not transmitted online, enter t

Strona 171 - Installing used tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 252 Exporting analysis data Proceed as follows:  Open the "Export

Strona 172 - Types of conditioning

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel involved with the instrument. Purpose This section describes the dialogs and co

Strona 173 - Flushing tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 254 Dialog descriptions key Element types The following list provid

Strona 174

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 255 File menu Purpose This section describes commands and dialogs f

Strona 175 - Performing the calibration

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 256 File > New (Command) What is the command used for? This comm

Strona 176 - Defining standard substances

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 257 Label Element type Meaning Mode Dropdown listbox Field in whi

Strona 177

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 258 Label Element type Meaning Signatures Listbox column Column d

Strona 178 - Requirements:

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 259 Further information Further information includes instructions i

Strona 179

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 26 Removing reaction tubes Please observe the following instructions: War

Strona 180

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 260 File > Delete (Command) What is the command used for? This c

Strona 181

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 261 Sign (Dialog) Function In the dialog:  the user is warned abo

Strona 182 - Displayed characteristics

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 262 Open You can open this dialog, if 21 CFR Part 11 functionality

Strona 183 - Coefficient "a"

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 263 Label Element type Meaning Cancel Button Aborts the process an

Strona 184

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 264 Open Open the dialog via: Menu command Button Hot key File >

Strona 185 - Calibration tables

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 265 Print (Dialog) Function In this dialog you can define print s

Strona 186 - Suggestion

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 266 Remaining elements: Label Element type Meaning OK Button Start

Strona 187 - Replacing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 267 Printer setup (Dialog) Function In this dialog you can specify

Strona 188 - Removing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 268 Open (Dialog) Function In this dialog you can specify the follo

Strona 189 - Top view furnace

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 269 Load balance file (Dialog) Function In this dialog you can sele

Strona 190

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 27 Warning Harmful substances when glass is broken! When filled quartz o

Strona 191 - Installing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 270 In section "Backup": Label Element type Meaning Selec

Strona 192

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 271 Clean database (Dialog) Function In the dialog:  the user is

Strona 193 - Replacing sealing elements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 272 Caution Data loss! Restoring the database via Restore irrevoca

Strona 194

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 273 Label Element type Meaning Cancel Button Aborts the process or

Strona 195 - Removing sealing elements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 274 Edit menu Purpose This section describes commands and dialogs f

Strona 196 - Ball valve maintenance

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 275 Edit > Redo (Command) What is the command used for? This com

Strona 197

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 276 Short cuts Invocation via the toolbar: Invocation via hot key

Strona 198

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 277 Short cuts Invocation via the toolbar: Note The line to delet

Strona 199 - Dismantled ball valve

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 278 If 21 CFR Part 11 functionality is enabled, a new version of th

Strona 200

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 279  by clicking the right mouse key to the corresponding sample

Strona 201

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 28 Overheating of tube fillings Please observe the following instruction:

Strona 202 - Requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 280 Note After invoking this command the dialog "Recalculate H

Strona 203

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 281 View menu Purpose This section describes commands and dialogs f

Strona 204

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 282 View > Toggle (Command) What is the command used for? This c

Strona 205

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 283 Elements The following describes the elements of the dialog. La

Strona 206

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 284 Elements The following describes the elements of the dialog. La

Strona 207

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 285 Load views (Dialog) Function In this dialog you can reload save

Strona 208

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 286 View > Gridview > Auto align (Command) What is the comman

Strona 209 - Installing the Ni flap

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 287 Further information Further information includes instructions i

Strona 210

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 288 Further information Further information includes instructions i

Strona 211

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 289 System menu Purpose This section describes commands and dialogs

Strona 212 - Installing the O

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel working with the instrument. Purpose This section provides general information

Strona 213

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 290 System > Auto run (Command) What is the command used for? Th

Strona 214

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 291 Note The "Abort analysis" dialog appears. Observe the

Strona 215

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 292 Label Element type Meaning Cancel Button Aborts the process. F

Strona 216

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 293 Label Element type Meaning Position Radiobutton Moves the car

Strona 217

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 294 Further information Further information includes instructions i

Strona 218 - Cleaning the carousel

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 295 Windows menu Purpose This section describes commands and dialog

Strona 219

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 296 Windows > Toolbar / Run-Bar (Command) What are these command

Strona 220

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 297 Icon Command Calibration > Next sample System > Wake-up

Strona 221 - Emptying reaction tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 298 Label Element type Meaning No. Label Displays the number of t

Strona 222 - Filling the combustion tube

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 299 Options menu Purpose This section describes commands and dialog

Strona 223

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 3 Copyright © BÜCHI Labortechnik AG All rights reserved This document contains propri

Strona 224 - Filling the reduction tube

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 30 Analytical characteristics and technical specifications Target group Perso

Strona 225

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 300 Maintenance intervals (Dialog) Function In this dialog, any num

Strona 226 - In this section

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 301 Further information Further information includes instructions i

Strona 227

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 302 Commands for the maintenance of the liquid sampler VLS Commands

Strona 228

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 303  Maintenance work to be performed by the customer (on page 16

Strona 229

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 304 In the lower area: Label Element type Meaning Result Label Th

Strona 230

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 305 Label Element type Meaning Apply Button Heats up the correspon

Strona 231

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 306 Remaining elements: Label Element type Meaning Close Button Cl

Strona 232

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 307 Open Open the dialog via:  Options > Diagnostics > Erro

Strona 233

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 308 Label Element type Meaning autom. Auto-increment the number in

Strona 234 - Filling the drying tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 309 Label Element type Meaning Name Textbox/label Field to input

Strona 235 - Drying tube filling (large)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 31 Analytical characteristics Analytical characteristics The following table

Strona 236

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 310 Further information Further information includes instructions i

Strona 237

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 311 Open Open the dialog via Options > Settings > Calculation

Strona 238

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 312  If you are using multiple analyzers with one PC, you must sp

Strona 239 - Repairing the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 313 In section "Network": Label Element type Meaning Path

Strona 240 - Interpreting error code

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 314 Valid for all tabs: Remaining elements: Label Element type Mean

Strona 241 - Performing a system test

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 315 Label Element type Meaning Peak anticipation Textbox Field to

Strona 242 - Performing a leak test

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 316 Label Element type Meaning O2 dosing time Textbox Field to in

Strona 243 - Replacing fuses

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 317 Elements The following describes the elements of the dialog. La

Strona 244 - Fuse holder

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 318 In section "Sleep": Label Element type Meaning Sleep

Strona 245

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 319 Monthly logbook (Dialog) Function This dialog contains records

Strona 246 - Phase 3: Insert fuses

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 32 Interfaces USB, RS232 /V24, Safety low voltage as per DIN IEC 380/VDE 080

Strona 247 - After a computer crash

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 320 Further information Further information includes instructions i

Strona 248 - Reacting to a power failure

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 321 Safety instruction Strictly observe the safety instruction &q

Strona 249

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 322 Entry Standard Description Parity N Defines the type of parity

Strona 250

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 323 The following table describes the entries under the "Syste

Strona 251 - Export for support

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 324 Label Element type Meaning OK Button Saves new settings Cancel

Strona 252 - Exporting analysis data

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 325 Math menu Purpose This section describes commands and dialogs f

Strona 253 - Menu and dialog descriptions

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 326 Math > Blank values > Calculate (Command) What is the com

Strona 254 - Dialog descriptions key

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 327  Routine measuring work (on page 56)  Types of blank value

Strona 255 - File menu

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 328 The dialog The appearance of the dialog depends on the selected

Strona 256 - File > New (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 329 Elements The following describes the elements of the dialog. La

Strona 257 - Listbox columns

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 33 Instrument design Target group Personnel involved with the instrument. Pur

Strona 258 - Select version (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 330 Math. > Recalculate (Command) What is the command used for?

Strona 259 - Save file as (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 331 Statistics menu Purpose This section describes commands and dia

Strona 260 - File > Delete (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 332 Statistics > Via names (Command) What is the command used fo

Strona 261 - Sign (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 333 Statistics > Include/Exclude sample (Command) What is the co

Strona 262 - Export to LIMS (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 334 Calibration menu Purpose This section describes commands and di

Strona 263 - Configure report (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 335 Calibration coefficients (Dialog) Function This dialog displays

Strona 264 - Further information

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 336 Label Element type Meaning Cancel Button Discards calibration

Strona 265 - Print (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 337 Further information Further information includes instructions i

Strona 266 - Print preview (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 338 Calibration > Next sample (Command) What is the command us

Strona 267 - Printer setup (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 339 Help menu Purpose This section describes commands and dialogs f

Strona 268 - Open (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 34 Front view Front view, closed The following picture shows the front view o

Strona 269 - Configure backup (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 340 Help > Content (Command) What is the command used for? This

Strona 270

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 341 In section "Analyzer": Label Element type Meaning Typ

Strona 272 - Log in as (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel involved with the instrument. In this chapter Warranty ...

Strona 273 - File > Exit (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 344 Warranty Target group Personnel involved with the instrument. In this section Warr

Strona 274 - Edit menu

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 345 Warranty of the overall instrument Warranty of the overall instrument Please refer

Strona 275 - Edit > Copy (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 346 Accessories, spare parts and consumables Target group Personnel involved with the i

Strona 276 - Edit > Paste (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 347 Smallest workable unit Condition You can only order the smallest workable unit if y

Strona 277 - Edit > Modify (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 348 Computer A computer is essential as the control and evaluation unit. The computer c

Strona 278 - Set stop tag (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 349 Consumables set for solid samples  Optional  Required when the material from th

Strona 279

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 35 Furnace section Location of the furnace section The furnace section is loc

Strona 281 - View menu

Operation Manual D-480 ©BÜCH Labortechnik AG Index 351 2 21 CFR Part 11 functionality - 73, 94, 259, 260, 261, 262, 320 A About this document - 15

Strona 282 - Configure view (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 352 Defining the balance / PC interface - 87 Defining the Kjeldahl factor - 132 Defining the LI

Strona 283 - Column properties (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 353 Loading a sample view - 150, 285 Log in as (Dialog) - 272 M Maintaining the instrument - 16

Strona 284 - Save views (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 354 Selecting the operating mode - 110, 131, 294 Set current weighed sample (Dialog) - 279 Set

Strona 286 - Function

Technical data are subject to change without notice/Quality Systems ISO 9001.The English version is the original language version and serves as basis

Strona 287

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 36 Top view furnace The following picture shows a top view of the furnace pul

Strona 288 - Select columns (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 37 Right side view Right side view, closed The following picture shows the ri

Strona 289 - System menu

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 38 Left side view Left side view, closed The following picture shows the left

Strona 290 - System > Stop (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 39 Top view Top view of the instrument The following picture shows the top vi

Strona 293 - Analysis mode (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with basic chemical knowledge and basic computer knowledge. Purpose This sectio

Strona 294

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 42 Layout and mode of functioning Target group

Strona 295 - Windows menu

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 43 Functional units Introduction The following

Strona 296 - Toolbar

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 44 I Mechanical sample insertion and O2 dosing

Strona 297 - Weighing window (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 45 6 Post combustion tube with tube filling 

Strona 298

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 46 Processes in the instrument during a measure

Strona 299 - Options menu

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 47 Sample insertion and initiation of measureme

Strona 300

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 48  Volatile halogen compounds are bound on s

Strona 301 - Replace part (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 49 Basic facts about working with the instrumen

Strona 302 - Leak test (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 5 Contents CHAPTER 1 General 13 Revision history ...

Strona 303

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 50 Setting device parameters About instrument p

Strona 304 - System test (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 51 Instrument equipment Combustion tube filling

Strona 305

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 52 Filling the post combustion tube The followi

Strona 306 - Error display (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 53  The daily factor for a measuring componen

Strona 307 - Input options (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 54 Linear calculation over the whole range The

Strona 308 - Standard samples (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 55 Polynomial calculation over the whole range

Strona 309 - Keywords (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 56 Computing calibration coefficients Once the

Strona 310 - Acoustic signals (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 57 Routine measuring work is performed at set i

Strona 311 - LIMS settings (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 58 Blank value determination In blank value det

Strona 312 - "LIMS data" tab

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 59 Understanding the operating software Target

Strona 313 - "Identifier" tab:

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 6 Understanding the operating software ...

Strona 314 - Device parameters (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 60 Basic functions of the operating software In

Strona 315 - Method (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 61 Software user interface The main window of t

Strona 316 - Error handling (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 62  ... display the online help. Details on t

Strona 317

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 63 View The sample view looks like a familiar c

Strona 318

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 64 Sample not yet analyzed, but a sample name

Strona 319 - Monthly logbook (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 65 Progression view (graph view) Progression v

Strona 320 - Select period (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 66 Statistics view The statistics view display

Strona 321 - "DEVICE.INI" tab

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 67 If your series includes samples previously d

Strona 322

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 68 The areas of the status view and what they m

Strona 323 - Configure key value (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 69 Copyright © BÜCHI Labortechnik AG All rights reserved This document contains propri

Strona 324

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 7 Start-up ...

Strona 325 - Math menu

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 70 In dialogs In dialogs you can also press the right mouse button to display certain

Strona 326 - Blank values (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 71 Data administration and data security Target group Personnel with basic chemical kn

Strona 327 - Define type of peak (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 72 Laboratory information and management system (LIMS) What does LIMS do? The Laborato

Strona 328 - Area assignment (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 73 21 CFR Part 11 functionality What is 21 CFR Part 11? 21 CFR Part 11 is a regulation

Strona 329

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 74 Restricted access to menu functions The software restricts access to the menu funct

Strona 330

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with good knowledge of the operating system and administrative settings. Purpos

Strona 331 - Statistics menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 76 Installing and updating the software Conditions for

Strona 332

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 77 Configure analyzer Target group Personnel with basi

Strona 333

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 78 What can you modify in the configuration? Safety

Strona 334 - Calibration menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 79 Creating new sections Safety instruction Strictly

Strona 335

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 8 Setting the size of the graph ...

Strona 336

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 80 Defining LIMS export settings Target group Personne

Strona 337

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 81 LIMS export settings What is set? The following are

Strona 338

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 82 Setting up user administration Target group Personn

Strona 339 - Help menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 83 User administration User groups Access to menu func

Strona 340 - Help > Find (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 84 Safety instruction Strictly observe the safety in

Strona 341 - Short cuts

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 85 Defining interfaces Target group Personnel with goo

Strona 342

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 86 Defining the analyzer / PC interface Note The opera

Strona 343 - Appendix

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 87 Defining the balance / PC interface Safety instru

Strona 344 - Warranty

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 88 Editing analysis data Target group Personnel with g

Strona 345 - Warranty on the furnace

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 89 When does it make sense to edit analysis data? Reas

Strona 346 - 11 - Appendix 346

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 9 Filling, removing and installing the absorption and drying tubes ...

Strona 347 - Required accessories

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 90 Performing checks Target group Personnel with good

Strona 348 - Optional accessories

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 91 Checking documents for authenticity What signature

Strona 349 - 11 - Appendix 349

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 92 Viewing the logbook Viewing the logbook Proceed a

Strona 350

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 93 Working with the database Target group Personnel wi

Strona 351 - Index 351

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 94 Database What is a database? A database is characte

Strona 352 - Index 352

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 95 Defining the autoexport directory Safety instruct

Strona 353 - Index 353

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 96 Autoexport Autoexport creates a backup of the curre

Strona 354 - Index 354

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 97 Reorganize database Proceed as follows:  Open the

Strona 355

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 98 Ways of optimizing the use of the analyzer Target g

Strona 356 - Find your BUCHI Contacts:

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 99 Optimizing basic instrument settings Analyzer confi

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